HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-tert-Butyl-N'-[2,6-di(butan-2-yl)phenyl]thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | HCID 20346983 | HCID 20346983 | — |
| Product | N-tert-Butyl-N'-[2,6-di(butan-2-yl)phenyl]thiourea | HCID 20347037 | — |
Reaction Steps
20.6 g of 2,6-di-sec.-butyl-phenyl isothiocyanate are dissolved in 20.0 g of tert.-butylamine and the batch is kept for 12 hours at 20° C. It is then poured into dilute hydrochloric acid and the reaction product is filtered off, washed until neutral and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04194008 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-18d5863ac5624e8da7056b87cf03180f |
| Source note | uspto-grants-1980_03 |