HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1701560Generated: October 26, 2026
2-Butanamine, 2-methyl- → N-(2,6-Diisopropyl-phenyl)-N'-tert.-pentyl-thiourea
https://huagongshe.com/reaction/1701560
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Butanamine, 2-methyl- | HCID 68986 | — |
| Reactant | 2-Isothiocyanato-1,3-bis(propan-2-yl)benzene | HCID 141194 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-(2,6-Diisopropyl-phenyl)-N'-tert.-pentyl-thiourea | HCID 20347005 | — |
Reaction Steps
11.0 g of 2,6-diisopropyl-phenyl isothiocyanate and 10 g of tert.-pentylamine are warmed with 5 ml of triethylamine for 10 minutes at 100°. After standing for 12 hours, the mixture which has partially crystallised out is stirred with petroleum ether and cooled to -10° C., and the product is filtered off and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04194008 |
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| Source dataset | uspto-grants-1980_03 |
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| ORD ID | ord-d9b862f4e5314eeca858816b39825fce |
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| Source note | uspto-grants-1980_03 |
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