Hydrochloric Acid → HCID 20346954, compound

Participants

Reaction Steps

15.0 g of 2,6-di-sec.-butyl-phenyl isothiocyanate are introduced, whilst cooling, into 20 g of a 65% strength aqueous solution of isopropylamine. After stirring for 3 hours at 20°, the batch is stirred into dilute hydrochloric acid, the reaction product which has precipitated in a crystalline form is filtered off and washed until neutral, and the paste is triturated with 50% strength methanol, again filtered off and dried.

Provenance & Evidence