Hydrochloric Acid → HCID 20347056, compound

Participants

Reaction Steps

20.0 g of cyclopentylamine are taken and 15.0 g of 2,6-di-sec.-butyl-phenyl isothiocyanate are introduced whilst stirring. The reaction takes place exothermically. The batch is left to stand for 12 hours and is then stirred with dilute hydrochloric acid and filtered. The filter cake is triturated with dilute methanol, filtered off, washed and dried. For further purification, the product can be recrystallised from petroleum ether. Yield 18 g; melting point 107°-108° C.

Provenance & Evidence