Dodecylamine → N-Dodecyl-2-(2-hydroxyethoxy)acetamide

HRID 1701725Notes

Reaction equation

HRID 1701725 reaction equation
[O:1]1[CH2:6][CH2:5][O:4][CH2:3][C:2]1=[O:7].[CH2:8]([NH2:20])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]>>[CH2:8]([NH:20][C:2](=[O:7])[CH2:3][O:4][CH2:5][CH2:6][OH:1])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

3

Reactant 2

HCID 13583DodecylamineHCID 18233Dioxanone

Product 1

HCID 54004293N-Dodecyl-2-(2-hydroxyethoxy)acetamide

Conditions

Temperature
100 °C

Procedure

In a glass reaction vessel 10.2 grams (0.1 mole) of 2-p-dioxanone was admixed with 18.5 grams (0.1 mole) of dodecyl amine and heated to 100° C. on a steam bath until reaction was completed within the period of 1 hour. The resulting liquid product was then poured on a glass plate and cooled to room temperature whereupon a pale yellow solid was formed. IR=6.06 mu.

Workup

  1. customwas completed within the period of 1 hour
  2. additionThe resulting liquid product was then poured on a glass plate
  3. temperaturecooled to room temperature whereupon a pale yellow solid
  4. customwas formed

Sources & evidence

ORD record
ord-fbdd30c4d7444972ab3653d11edd8ce7
Source dataset
uspto-grants-1980_03
Patent number
US04195096

Reaction notes

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