HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178482391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 178506455 | HCID 178506455 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178482391 | HCID 178482391 | 20.3% |
Reaction Steps
500 mg of (E)-5-(indol-3-ylmethylene)-1,3-dimethyl-2-imino-4-imidazolidinone are refluxed in methanol for 24 hours with 425 mg of methyl iodide. The product is chromatographed on silica gel and alumina. There are obtained 107 mg of (E)-5-(indol-3-ylmethylene)-1,3-dimethyl-2-methylimino-4-imidazolidinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04195179 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-84c3523a74dc40eb901cdaaae79c039e |
| Source note | uspto-grants-1980_03 |