HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorobenzoic acid → 2-Fluorobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorobenzoic acid | HCID 9935 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-Fluorobenzoyl chloride | HCID 9808 | — |
Reaction Steps
A mixture of 14.0 g (0.1 mole) of 2-fluorobenzoic acid and 30 ml of thionyl chloride (SOCl2) is refluxed in 70 ml of benzene for four hours. The mixture is cooled and concentrated under vacuum to give 2-fluorobenzoyl chloride as a liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04195023 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-2f2fd7cdc15b4ed6bd2ac0e8ccccc61c |
| Source note | uspto-grants-1980_03 |