HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 15583064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | HCID 15583071 | HCID 15583071 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15583064 | HCID 15583064 | — |
Reaction Steps
A solution of 14.5 g of 3-[2-(cyclohexyloxy)-ethoxy]aniline in 100 ml of toluene was added dropwise to 100 ml of toluene containing 12 g of phosgene. The resultant mixture was refluxed for 1 hour and concentrated under reduced pressure. The concentrate was purified by high vacuum distillation to give 14 g of 3-[2-(cyclohexyloxy)-ethoxy]phenyl isocyanate. B.P., 112°-115° C./0.06 mmHg. nD23 1.5283.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04378992 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-3f3b620245124fe7a4b796df57d77ec3 |
| Source note | uspto-grants-1983_04 |