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HRID1701833

反应详情

EQUATION

反应方程式

HRID 1701833 的结构方程式

REACTANTS

反应物

2
结构：Nc1ncc([N+](=O)[O-])s1
HCID8486

2-Amino-5-nitro-1,3-thiazole

C3H3N3O2S

结构：O=C(Cl)c1cccc([N+](=O)[O-])c1
HCID8495

3-Nitrobenzoyl chloride

C7H4ClNO3

PRODUCTS

生成物

1
结构：O=C(Nc1ncc([N+](=O)[O-])s1)c1cccc([N+](=O)[O-])c1
HCID298930

MLS000756380

C10H6N4O5S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

By following the procedure of the first part of Example 1, but using m-nitrobenzoyl chloride (27.8 g), 2-amino-5-nitrothiazole (21.8 g) and pyridine (100 ml), there was obtained 3-nitro-N-(5-nitro-2-thiazolyl)benzamide, m.pt 200°-201°, after recrystallisation from acetic acid.