HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-Nitrothiazole → 3-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-Nitrothiazole | HCID 8486 | — |
| Reactant | Benzoyl chloride, 3-nitro- | HCID 8495 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 3-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide | HCID 298930 | — |
Reaction Steps
By following the procedure of the first part of Example 1, but using m-nitrobenzoyl chloride (27.8 g), 2-amino-5-nitrothiazole (21.8 g) and pyridine (100 ml), there was obtained 3-nitro-N-(5-nitro-2-thiazolyl)benzamide, m.pt 200°-201°, after recrystallisation from acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379156 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-869f3175addf4932a6aa8edebdad26e4 |
| Source note | uspto-grants-1983_04 |