HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-Nitrothiazole → HCID 3422255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-Nitrothiazole | HCID 8486 | — |
| Reactant | 2-Chlorobenzoyl chloride | HCID 69110 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 3422255 | HCID 3422255 | — |
Reaction Steps
By following the procedure of the first part of Example 1, but using 2-chlorobenzoyl chloride (26.3 g), 2-amino-5-nitrothiazole (21.8 g) and pyridine (ca 150 ml), there was obtained 2-chloro-N-(5-nitro-2-thiazolyl)benzamide, m.pt 221°-222°, after recrystallisation from acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379156 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-d82ecbc0ea774d5eaefeeb78a6be646b |
| Source note | uspto-grants-1983_04 |