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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1701840Generated: October 31, 2026

2,2,2-Trifluoroethyl trichloromethanesulphonate → HCID 13116877, compound

https://huagongshe.com/reaction/1701840

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,2,2-Trifluoroethyl trichloromethanesulphonateHCID 90027—
ReactantHCID 178527834HCID 178527834—
ProductHCID 13116877HCID 13116877—

Reaction Steps

By the procedure described in Example 1, 2.0 g of 4,5-bis-(4-chlorophenyl)-4,5-dihydro-1H-imidazole-2-thiol was reacted with 2,2,2-trifluoroethyl trichloromethanesulfonate to give the title compound. Recrystallization from nitromethane afforded 850 mg of colorless crystals, m.p. 230° dec. The NMR and infrared spectra were consistent with this structure.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04379159
Source datasetuspto-grants-1983_04
ORD IDord-adf3cc61b0a549a9a8f82b637e080778
Source noteuspto-grants-1983_04