HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 12875799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 12853022 | HCID 12853022 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12875799 | HCID 12875799 | — |
Reaction Steps
Ethyl 3-(2-pyridylmethylthio)propionimidate was reacted with an equimolar amount of ammonium chloride in methanol for 2 hours at room temperature and the product was recrystallized from a mixture of ethanol and ether to provide 3-(2-pyridylmethylthio)propionamidine dihydrochloride showing a melting point of 140°-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379158 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-cc53ab4d0ef64adaacbd2b74b7d34ce4 |
| Source note | uspto-grants-1983_04 |