HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13207837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22822903 | HCID 22822903 | — |
| Product | HCID 13207837 | HCID 13207837 | — |
Reaction Steps
Thionyl chloride (300 g) was slowly added to 3-(3,5-cis-dimethylpiperazino)propanol dihydrochloride (200 g). The reaction was gently refluxed for an hour followed by removal of excess thionyl chloride by vacuum distillation. The resulting solid was washed with several portions of benzene then several portions of ether, m.p. 291°-292°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379160 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-56c97d571e034ae4a2f50aac9b873653 |
| Source note | uspto-grants-1983_04 |