Thionyl Chloride → HCID 20505264, compound

HRID 1701856Notes

Reaction equation

HRID 1701856 reaction equation
[C:1]1([CH2:7][N:8]2[CH2:12][CH2:11][CH2:10][CH:9]2[CH2:13][CH2:14][OH:15])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.S(Cl)([Cl:18])=O>C(Cl)(Cl)Cl>[C:1]1([CH2:7][N:8]2[CH2:12][CH2:11][CH2:10][CH:9]2[CH2:13][CH:14]([Cl:18])[OH:15])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 13507086HCID 13507086, compound

Product 1

HCID 20505264HCID 20505264, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

17.8 g of 2-[1-(1-cyclohexenylmethyl) 2-pyrrolidinyl]ethanol (0.085 mole) and 50 ml of chloroform are introduced into a 250 ml balloon flask provided with a stirrer, a thermometer, a condenser and a dropping funnel, then 15.3 ml of thionyl chloride is dropped in, the temperature being kept at about 25°-25° C. by cooling.

Workup

  1. customprovided with a stirrer
  2. custombeing kept at about 25°-25° C.
  3. temperatureby cooling

Sources & evidence

ORD record
ord-34ec5c41088649af941509588eead429
Source dataset
uspto-grants-1983_04
Patent number
US04379161

Reaction notes

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