HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20505264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13507086 | HCID 13507086 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20505264 | HCID 20505264 | — |
Reaction Steps
17.8 g of 2-[1-(1-cyclohexenylmethyl) 2-pyrrolidinyl]ethanol (0.085 mole) and 50 ml of chloroform are introduced into a 250 ml balloon flask provided with a stirrer, a thermometer, a condenser and a dropping funnel, then 15.3 ml of thionyl chloride is dropped in, the temperature being kept at about 25°-25° C. by cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379161 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-34ec5c41088649af941509588eead429 |
| Source note | uspto-grants-1983_04 |