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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1701861Generated: November 4, 2026

1,3-Propanedithiol → HCID 18628082, compound

https://huagongshe.com/reaction/1701861

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-PropanedithiolHCID 8013—
ReactantTriethylamineHCID 8471—
ReactantHCID 53695827HCID 53695827—
SolventMethanolHCID 887—
ProductHCID 18628082HCID 18628082—

Reaction Conditions

Temperature0 °C

Reaction Steps

Stir the product of Step C (49.5 g, 0.22 mole), 1,3-propane dithiol (103.6 g, 0.96 mole) and triethylamine (101.0 g, 1.0 mole) in methanol (1500 ml) for 72 hours. Cool to 0° C., filter and evaporate in vacuo to obtain 2-amino-1-(4-hydroxy-3-methylthiophenyl)ethanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04379166
Source datasetuspto-grants-1983_04
ORD IDord-88f3ffa415a34a7fa6829424a947f7cb
Source noteuspto-grants-1983_04