HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 12953404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 12953392 | HCID 12953392 | — |
| Product | HCID 12953404 | HCID 12953404 | — |
Reaction Steps
Ethyl 2-(3-bromophenyl)-4-thiazolylacetate prepared by the process in Example 2 (10 g) in 75 ml of 28% NH4OH was stirred at room temperature. About 10 ml of dioxane was added to facilitate mixing. After 10 days, the crystalline product was filtered. The yield of product was 8.3 g, mp 150°-152° C. When recrystallized from alcohol, it melted 152°-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379791 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-d1921305343c483f85d27b7b67a0bc2e |
| Source note | uspto-grants-1983_04 |