HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 15580738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Amino-3-methoxybenzoic acid | HCID 255720 | — |
| Reactant | p-Acetoxybenzoyl chloride | HCID 2756254 | — |
| Product | HCID 15580738 | HCID 15580738 | — |
Reaction Steps
16.7 gm (0.1 mol) of 3-methoxy-anthranilic acid were dissolved in 100 ml of pyridine, and the solution was mixed, while cooling and stirring, with 23.8 gm (0.1 mol+20%) of 4-acetoxy-benzoyl chloride. After 2 hours the reaction was finished, and the reaction mixture was poured into ice water. The crystalline precipitate thus formed was suction filtered off, dried and recrystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379788 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-87d3a34174fe4828b8e5b725614a0fee |
| Source note | uspto-grants-1983_04 |