1-Bromo-4-chlorobutane → HCID 13072454, compound

Participants

Reaction Steps

4 gm (0.014 mol) of the product in (b) were dissolved in 30 ml of dimethylsulfoxide, and the solution was mixed, while stirring, with 1.75 gm (0.014 mol+10%) of potassium tert. butylate. Subsequently, 4 ml of 1-bromo-4-chlorobutane were added, and the reaction mixture was stirred at room temperature until the reaction was complete. The reaction mixture was poured into ice water, and the crystalline precipitate thus formed was suction-filtered off, washed well with water and dried.

Provenance & Evidence