HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-Aminopropyl)morpholine → HCID 53688069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-Aminopropyl)morpholine | HCID 61055 | — |
| Reactant | 3-Morpholinopropanal | HCID 11105482 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 53688069 | HCID 53688069 | — |
Reaction Steps
143 g (1 mol) of 3-morpholinopropionaldehyde in 143 g of dioxane are pumped into 72 g (0.5 mol) of aminopropylmorpholine and 30 g of Raney nickel at 120° C. and hydrogenated at 180 bar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379861 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-81fdeffed5ed4be7a4a704a451bbe4bf |
| Source note | uspto-grants-1983_04 |