HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 2,2-Dimethyl-4-(1,2,4-triazol-1-yl)-6-phenoxy-hexan-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Reactant | 3,3-Dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone | HCID 100877 | — |
| Product | 2,2-Dimethyl-4-(1,2,4-triazol-1-yl)-6-phenoxy-hexan-3-one | HCID 12806680 | — |
Reaction Steps
2.6 g of sodium hydride, 16.7 g of 2,2-dimethyl-4-(1,2,4-triazol-1-yl)-butan-3-one and 20.1 g of 1-bromo-2-phenoxyethane are reacted by a method similar to that of Example 1b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04380546 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-ae3f0af5cd3b42d986a1b3b1dd0066f5 |
| Source note | uspto-grants-1983_04 |