Methylamine → HCID 178482525, compound

HRID 1702284Notes

Reaction equation

HRID 1702284 reaction equation
CO[C:3]1[C:7](OC)=[N:6][S:5](=[O:11])(=[O:10])[N:4]=1.[CH3:12][C:13]1[O:17][N:16]=[C:15]([CH2:18][S:19][CH2:20][CH2:21][NH2:22])[N:14]=1.[CH3:23][NH2:24]>>[CH3:12][C:13]1[O:17][N:16]=[C:15]([CH2:18][S:19][CH2:20][CH2:21][NH:22][C:7]2[C:3]([NH:24][CH3:23])=[N:4][S:5](=[O:10])(=[O:11])[N:6]=2)[N:14]=1

Participants

4

Reactant 3

HCID 6329MethylamineHCID 122305383,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxideHCID 155923022-[(5-Methyl-1,2,4-oxadiazol-3-yl)methylthio]ethylamine

Product 1

HCID 178482525HCID 178482525, compound

Procedure

When a methanolic suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is treated successively with 2-[(5-methyl-1,2,4-oxadiazol-3-yl)methylthio]ethylamine [prepared in Step A] and methylamine, by the general procedure of Example 2, the title compound is thereby produced.

Sources & evidence

ORD record
ord-a385390492ff49fbb030f3165605147e
Source dataset
uspto-grants-1983_04
Patent number
US04380638

Reaction notes

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