HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20503815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20503814 | HCID 20503814 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20503815 | HCID 20503815 | — |
Reaction Steps
Prepared analogously to Example 6 from 9-(n-butyl)-1,3-dimethyl-1,4,9,10-tetrahydro-pyrazolo[4,3-e]pyrido[3,2-b][1,4]diazepin-10-one, sodium hydride, and methyl iodide in N,N-dimethylformamide with subsequent chromatographic purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04381303 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-0569121c30ea4feabec3621dbd521e19 |
| Source note | uspto-grants-1983_04 |