HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 12923102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Acetylthiourea | HCID 2723593 | — |
| Reactant | HCID 13050589 | HCID 13050589 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12923102 | HCID 12923102 | 65.6% |
Reaction Steps
A 1.0 g portion of 4-(4-chlorobenzyloxy)phenacyl chloride, together with 440 mg of 1-acetylthiourea and 279 mg of sodium acetate, was stirred in 15 ml of ethanol under reflux for 2 hours. After cooling, the precipitated crystals were recovered by filtration, thus yielding 800 mg (65.6%) of 2-acetylamino-4-[4-(4-chlorobenzyloxy)phenyl]thiazole. m.p., 239°-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348403 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-5de4f27baf6a439794358f3d018bc890 |
| Source note | uspto-grants-1982_09 |