HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20525799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 53804060 | HCID 53804060 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20525799 | HCID 20525799 | — |
Reaction Steps
A mixture of 5 g. of methyl (4-hexadecylaminophenyl)pyruvate, 5 g. of potassium hydroxide and 50 ml. of a 1:1 ethanol:water solution is heated to 50° for 3 hrs. While hot, the reaction mixture is neutralized with acetic acid and cooled. The precipitate is collected, dried and recrystallized, yielding (4-hexadecylaminophenyl)pyruvic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348399 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-e131551a74294ddc829f34303a545224 |
| Source note | uspto-grants-1982_09 |