HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycol monoethyl ether → HCID 20525890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycol monoethyl ether | HCID 8076 | — |
| Reactant | HCID 20525783 | HCID 20525783 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20525890 | HCID 20525890 | — |
Reaction Steps
Prepared as described in Example 18, 10.0 g. of 4-(hexadecylamino)hydrocinnamoyl chloride hydrochloride in 80. ml. of methylene chloride is treated with 9.5 g. of 4-dimethylaminopyridine and 2.1 g. of 2-ethoxyethanol, analogous to the method of Example 19. Workup and filtration through alumina provides 2-ethoxyethyl 4-(hexadecylamino)hydrocinnamate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348399 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-db7b1ffb1f6b48ac9fceb73b5cb13496 |
| Source note | uspto-grants-1982_09 |