HRID1702685

反应详情

EQUATION

反应方程式

HRID 1702685 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 2-phenyl-1,3-dioxan-5-yl 4-(hexadecylamino)hydrocinnamate, 10% palladium-on-carbon and acetic acid is treated with hydrogen in a Parr apparatus at room temperature until hydrogen uptake ceases. The mixture is filtered and the filtrate is evaporated. Recrystallization of the residue from chloroform provides the title compound.

WORKUP

后处理

  1. filtrationThe mixture is filtered
  2. customthe filtrate is evaporated
  3. customRecrystallization of the residue from chloroform