HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenyl-1,3-dioxan-5-yl 4-(hexadecylamino)hydrocinnamate → 2-Hydroxy-1-(hydroxymethyl)ethyl 4-(hexadecylamino)hydrocinnamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenyl-1,3-dioxan-5-yl 4-(hexadecylamino)hydrocinnamate | HCID 53632723 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-Hydroxy-1-(hydroxymethyl)ethyl 4-(hexadecylamino)hydrocinnamate | HCID 54087480 | — |
Reaction Steps
A mixture of 2-phenyl-1,3-dioxan-5-yl 4-(hexadecylamino)hydrocinnamate, 10% palladium-on-carbon and acetic acid is treated with hydrogen in a Parr apparatus at room temperature until hydrogen uptake ceases. The mixture is filtered and the filtrate is evaporated. Recrystallization of the residue from chloroform provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348399 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-725f4360b40c430493054031178b1f00 |
| Source note | uspto-grants-1982_09 |