Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 3-(Bicyclo[2.2.1]hept-5-en-2-yl)prop-2-enoic acid | HCID 85819 | — |
| Reactant | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Product | HCID 54493129 | HCID 54493129 | — |
Reaction Steps
Diphenylphosphoryl azide (12.1 g.) was added dropwise to a solution of 3-(5-norbornen-2-yl)acrylic acid (6.57 g.) in dry pyridine (30 ml.) and stirred at 80° C. for 30 minutes to give 2-(5-norbornen-2-yl)ethenyl isocyanate (I.R.: 2260 cm-1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04349552 |
|---|
| Source dataset | uspto-grants-1982_09 |
|---|
| ORD ID | ord-f245594fd0844007a5b92c5ce56aaf24 |
|---|
| Source note | uspto-grants-1982_09 |
|---|
