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Ethyl 7-chloroheptanoate → 7-[3-(4-Chlorophenyl)-2-oxo-4-phenyl-4-imidazolin-1-yl] enanthic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 7-chloroheptanoate | HCID 529988 | — |
| 反応物 | 1-(4-Chlorophenyl)-5-phenyl-4-imidazolin-2-one | HCID 12418988 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 7-[3-(4-Chlorophenyl)-2-oxo-4-phenyl-4-imidazolin-1-yl] enanthic acid ethyl ester | HCID 53657701 | — |
反応手順
The product is obtained as described in example 1 from 1.35 g NaJ (80% suspension in mineral oil), 12.2 g of 1-(4-chlorophenyl)-5-phenyl-4-imidazolin-2-one, 100 cc. of DMF, 8.7 g of 7-chloroenanthic acid ethyl ester and 1.35 g of NaJ. Eluant in chromatographic purification: hexane/ethyl acetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04349684 |
| 出典データセット | uspto-grants-1982_09 |
| ORD ID | ord-70babe5b36c84ee19e60180bfe43ff58 |
| 出典メモ | uspto-grants-1982_09 |