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HRID1702881

反应详情

EQUATION

反应方程式

HRID 1702881 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)CCCCCCCl
HCID529988

ethyl 7-chloroheptanoate

C9H17ClO2

结构：O=c1[nH]cc(-c2ccccc2)n1-c1ccc(Cl)cc1
HCID12418988

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CCCCCCn1cc(-c2ccccc2)n(-c2ccc(Cl)cc2)c1=O
HCID53657701

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The product is obtained as described in example 1 from 1.35 g NaJ (80% suspension in mineral oil), 12.2 g of 1-(4-chlorophenyl)-5-phenyl-4-imidazolin-2-one, 100 cc. of DMF, 8.7 g of 7-chloroenanthic acid ethyl ester and 1.35 g of NaJ. Eluant in chromatographic purification: hexane/ethyl acetate.

WORKUP

后处理

  1. customThe product is obtained
  2. customEluant in chromatographic purification