HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 54464238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Reactant | HCID 12418987 | HCID 12418987 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54464238 | HCID 54464238 | — |
Reaction Steps
The product is produced as described in example 1 from 2.4 g of NaH (80% suspension in mineral oil), 21.3 g of 1-(4-methoxyphenyl)-5-phenyl-4-imidazolin-2-one, 160 cc. of DMF 19 g of 8-bromocaprylic acid methyl ester and 2.4 g of NaJ. Eluant in chromatographic purification: hexane/ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04349684 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-bafcbc20f8a4461eb750a414a7887afd |
| Source note | uspto-grants-1982_09 |