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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1702890Generated: October 30, 2026

Sodium hydride → HCID 53986850, compound

https://huagongshe.com/reaction/1702890

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium hydrideHCID 24758—
ReactantHCID 10037742HCID 10037742—
ReactantMethyl 8-bromooctanoateHCID 11107373—
SolventDimethylformamideHCID 6228—
ProductHCID 53986850HCID 53986850—

Reaction Steps

The product is produced as described in example 1 from 1.8 g of NaH (80% suspension in mineral oil), 15 g of 1-benzyl-5-phenyl-4-imidazolin-2-one, 120 cc. of DMF, 14.2 g of 8-bromocaprylic acid methyl ester and 1.8 g of NaJ.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04349684
Source datasetuspto-grants-1982_09
ORD IDord-897b18ec15154767aa34fb6088d9f2f4
Source noteuspto-grants-1982_09