HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 54448380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1,4,5-Triphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 628544 | — |
| Reactant | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54448380 | HCID 54448380 | — |
Reaction Steps
The product is produced as described in example 1 from 1.2 g of NaH (80% suspension in mineral oil), 12 g of 1.4.5-triphenyl-4-imidazolin-2-one, 80 cc. of DMF, 9.5 g of 8-bromocaprylic acid methyl ester and 1.2 g of NaJ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04349684 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-bbc9fc1d55304cbb9162f34e39c4414c |
| Source note | uspto-grants-1982_09 |