HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 53902604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Reactant | HCID 20525409 | HCID 20525409 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53902604 | HCID 53902604 | — |
Reaction Steps
The product is produced as described in example 1 from 0.63 of NaH (80% suspension in mineral oil), 5.9 g of 4.5-bis-(2-fluorophenyl)-1-methyl-4-imidazolin-2-one, 40 cc. of DMF, 5.0 g of 8-bromo caprylic methyl ester and 0.63 g of NaJ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04349684 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-440bf5b228934c0cb342e6f067dccbc3 |
| Source note | uspto-grants-1982_09 |