HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 11-(3-Ethyl-4.5-diphenyl-2-oxo-4-imidazolin-1-yl) undecanoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methyl 11-bromoundecanoate | HCID 223913 | — |
| Reactant | 1-ethyl-4,5-diphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 12675126 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 11-(3-Ethyl-4.5-diphenyl-2-oxo-4-imidazolin-1-yl) undecanoic acid methyl ester | HCID 53923526 | — |
Reaction Steps
The product is produced as described in example 1 from 0.45 g of NaH (80% suspension in mineral oil), 4 g of 1-ethyl-4.5-diphenyl-4-imidazolin-2-one, 30 cc. of DMF, 4.2 g of 11-bromoundecanoic acid methyl ester and 0.45 g of NaJ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04349684 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-acbf12d29ed64f7e901fcc2f4c3f7fac |
| Source note | uspto-grants-1982_09 |