HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 12961712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12961708 | HCID 12961708 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12961712 | HCID 12961712 | — |
Reaction Steps
13.6 g of [3-(4-chlorophenyl)-2-oxo-4-phenyl-4-imidazolin-1-yl] acetic acid ethyl ester and 1.52 g of NaOH are dissolved in 80 cc. of ethanol and the mixture is stirred at room temperature for 24 hours. The alcohol is distilled off in a vacuum and the residue is dissolved in water. The aqueous solution is shaken with ether, the aqueous phase is acidified with dilute hydrochloric acid and the precipitated acid is separated and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04349684 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-5926d80d62e249f7b26a5b19161b696b |
| Source note | uspto-grants-1982_09 |