Tetrahydrofuran → HCID 22761659, compound

Participants

Reaction Steps

The starting material is prepared as follows: The solution of 2 g of N-(4-nitro-2-iodomethylphenyl)-4-chlorophthalimide in 40 ml of tetrahydrofuran and 40 ml of methanol, is treated with 8.7 g of freshly prepared silver carbonate for 20 hours, with protection from light. The mixture is filtered and the filtrate evaporated, to yield the N-(2-methoxymethyl-4-nitrophenyl)-4-chlorophthalimide melting at 125°-128°.

Provenance & Evidence