Hydroxyamine hydrochloride → HCID 54314493, compound

Participants

Reaction Steps

The above-named compound was prepared from 2-(2-ethyl-3-benzofuranyl)-2-methyl-propionitrile by the procedure described in Example 1(a), but using 1.5 mol of hydroxylamine hydrochloride and sodium methylate for each mole of 2-(2-ethyl-3-benzofuranyl)-2-methylpropionitrile and continuing the reaction for 72 hours. Yield: 41%; m.p. 118°-120° C. after recrystallization from a mixture of ethyl acetate and light petroleum ether.

Provenance & Evidence