4-[(4-Chlorophenyl)sulfanyl]butanoic acid → HCID 23711742, compound

HRID 1703544Notes

Reaction equation

HRID 1703544 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13])=[CH:4][CH:3]=1.C[O-].[Na+:17]>C(O)(C)C>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH2:9][CH2:10][CH2:11][C:12]([O-:14])=[O:13])=[CH:4][CH:3]=1.[Na+:17]

Participants

4

Reactant 2

HCID 23071444-[(4-Chlorophenyl)sulfanyl]butanoic acidHCID 10942334Sodium Methoxide

Product 1

HCID 23711742HCID 23711742, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

A hot solution of 13.8 g of 4-(p-chlorophenylthio)butyric acid was added to a hot solution of 3.2 g of sodium methoxide in 50 ml of isopropanol. The resulting mixture was cooled and filtered. The air-dried solid weighed 14.4 g.

Workup

  1. temperatureThe resulting mixture was cooled
  2. filtrationfiltered

Sources & evidence

ORD record
ord-a363870edf5a4bd18e154adc038848db
Source dataset
uspto-grants-1978_11
Patent number
US04124723

Reaction notes

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