Diphenyl Ether → 6-Methoxymethyl-imidazo[1,5-d]-as-triazin-4(3H)-one

HRID 1703688Notes

Reaction equation

HRID 1703688 reaction equation
C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[C:10]([CH2:13][O:14][CH3:15])[NH:11][CH:12]=1)C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:15][O:14][CH2:13][C:10]1[N:9]2[C:4](=[O:3])[NH:5][N:6]=[CH:7][C:8]2=[CH:12][N:11]=1

Participants

3

Reactant 2

HCID 7583Diphenyl EtherHCID 1784735823-[2-(Methoxymethyl)-4-imidazolyl]methylene carbazic acid ethyl ester

Product 1

HCID 124933056-Methoxymethyl-imidazo[1,5-d]-as-triazin-4(3H)-one

Procedure

A mixture of 25.9 gm. of 3-{[2-(methoxymethyl)-4-imidazolyl]methylene}carbazic acid ethyl ester and 125 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product, m.p. 200°-205° C.

Workup

  1. additionA mixture of 25.9 gm

Sources & evidence

ORD record
ord-d508c5be89e14c048035ebea2d0c31ef
Source dataset
uspto-grants-1978_11
Patent number
US04124766

Reaction notes

Loading…