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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1703709Generated: October 31, 2026

Thiomorpholine → HCID 20505943, compound

https://huagongshe.com/reaction/1703709

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThiomorpholineHCID 67164—
Reactant2-Bromo-5-(chlorosulfonyl)benzoic acidHCID 3427298—
SolventDichloromethaneHCID 6344—
ProductHCID 20505943HCID 20505943—

Reaction Steps

This product is prepared by the reaction of 2-bromo-5-chlorosulfonyl benzoic acid with excess thiomorpholine in methylene chloride. The product, m.p. 195°-197.5° C., is purified by solution in aqueous sodium hydroxide, crystallization by acidifying the basic solution, and recrystallization from acetone-hexane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04124590
Source datasetuspto-grants-1978_11
ORD IDord-5fdff6eaaf9943609da3ca36ba279ae2
Source noteuspto-grants-1978_11