Hydrogen Bromide → HCID 86736144, compound

Participants

Reaction Steps

104 g of p-iodophenethyl alcohol was combined in solution with 216 g of hydrobromic acid (48%) and 36 g of thiourea in 100 ml of water and reacted in accordance with the procedure outlined in Example I(a). Vacuum distillation at 91°-95° and 0.2 mm Hg gave a 27% yield of p-iodophenethyl thiol having a refractive index of n25D = 1.6411, an ALD of 0.56 ml/Kg and a formula of C8H8IS.

Provenance & Evidence