Ethanol → HCID 86736149, compound

Participants

Reaction Steps

A solution of 80 grams (0.188 mole) of the product of Example 1 is dissolved in 2400 mls. of ethyl alcohol and made alkaline to phenolphthalein indicator paper by adding concentrated ammonium hydroxide thereto. The solution is cooled in an ice bath and diluted with 1200 mls. of ice (5° C.) water. The resulting precipitate is separated by filtration and dried in a vacuum oven to obtain 48 grams of product. This free base is believed to be a new compound and is claimed as such herein.

Provenance & Evidence