HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → HCID 22760815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | 1-(3-Chlorophenoxy)-3-sulfanylpropan-2-ol | HCID 12822264 | — |
| Product | HCID 22760815 | HCID 22760815 | — |
Reaction Steps
Analogously to Example 1, from maleic acid anhydride and 2-hydroxy-3-m-chlorophenoxypropane-1-thiol in the presence of diisopropylamine and the usual working up of the reaction mixture, 6-m-chlorophenoxymethyl-2-oxo-1,4-oxathiane-3-acetic acid is obtained. It is separated into two isomers using chromatographic purification:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125622 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-f7f8274833e141c2aca26861a7516e55 |
| Source note | uspto-grants-1978_11 |