huagongshe.com
HRID1703849

反应详情

EQUATION

反应方程式

HRID 1703849 的结构方程式

REACTANTS

反应物

2
结构：CCCCNC(=S)NCCCC
HCID2723622

N,N'-Dibutylthiourea

C9H20N2S

结构：NS(=O)(=O)c1cc(C(=O)CCl)ccc1Cl
HCID21316749

未命名化合物

PRODUCTS

生成物

1
结构：CCCCN=C1SCC(O)(c2ccc(Cl)c(S(N)(=O)=O)c2)N1CCCC.Cl
HCID22760688

未命名化合物

PROCEDURE

实验过程

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether. Colorless crystalline solid body: melting point: 164° C. (decomposition).

WORKUP

后处理

  1. customthe end product was precipitated with diisopropyl ether