HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dibutylthiourea → 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dibutylthiourea | HCID 2723622 | — |
| Reactant | 2,4'-Dichloro-3'-sulfamoylacetophenone | HCID 21316749 | — |
| Product | 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride | HCID 22760688 | — |
Reaction Steps
5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether. Colorless crystalline solid body: melting point: 164° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-ece374374bfd4becb56291145e59552d |
| Source note | uspto-grants-1978_11 |