反应详情

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 2.5 g of 1,3-diallyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diisopropyl ether and the oil obtained was crystallized with diethyl ether/ethyl acetate (1:1). Colorless solid body: melting point: 158° C. (decomposition).

1. customthe end product was precipitated with diisopropyl ether
2. customthe oil obtained
3. customwas crystallized with diethyl ether/ethyl acetate (1:1)