HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea, N,N'-di-2-propen-1-yl- → HCID 22760653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea, N,N'-di-2-propen-1-yl- | HCID 3034186 | — |
| Reactant | 2,4'-Dichloro-3'-sulfamoylacetophenone | HCID 21316749 | — |
| Product | HCID 22760653 | HCID 22760653 | — |
Reaction Steps
5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 2.5 g of 1,3-diallyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diisopropyl ether and the oil obtained was crystallized with diethyl ether/ethyl acetate (1:1). Colorless solid body: melting point: 158° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-0fc330388603408fa951e9a1a3be8ed8 |
| Source note | uspto-grants-1978_11 |